Preclinical evaluation of novel synthesised nanoparticles based on tyrosine poly(ester amide) for improved targeted pulmonary delivery.


Journal

Scientific reports
ISSN: 2045-2322
Titre abrégé: Sci Rep
Pays: England
ID NLM: 101563288

Informations de publication

Date de publication:
29 04 2024
Historique:
received: 10 02 2024
accepted: 12 04 2024
medline: 30 4 2024
pubmed: 30 4 2024
entrez: 29 4 2024
Statut: epublish

Résumé

Fixed dose combinations (FDCs) incorporating two or three medicines in a single inhaler have been created to enhance patient compliance and hence clinical outcomes. However, the development of dry powder inhalers (DPIs), particularly for FDCs, faces challenges pertinent to formulation uniformity and reproducibility. Therefore, this project aimed to employ nanotechnology to develop a FDC of DPIs for market-leading medicines-fluticasone propionate (FP) and salmeterol xinafoate (SAL)-for asthma management. Nanoaggregates were prepared using a novel biocompatible and biodegradable poly(ester amide) based on the amino acid tyrosine, utilising a one-step interfacial polymerisation process. The produced tyrosine poly (ester amide) drug-loaded nanoparticles were evaluated for content uniformity, PSA, FTIR, TEM, DSC, XRD and aerodynamic performance (in vitro and in vivo). The optimised formulation demonstrated high entrapment efficiency- > 90%. The aerodynamic performance in terms of the emitted dose, fine particle fraction and respirable dose was superior to the carrier-based marketed product. In-vivo studies showed that FP (above the marketed formulation) and SAL reached the lungs of mice in a reproducible manner. These results highlight the superiority of novel FDC FP/SAL nanoparticles prepared via a one-step process, which can be used as a cost-effective and efficient method to alleviate the burden of asthma.

Identifiants

pubmed: 38684750
doi: 10.1038/s41598-024-59588-1
pii: 10.1038/s41598-024-59588-1
doi:

Substances chimiques

Tyrosine 42HK56048U
Polyesters 0
Fluticasone CUT2W21N7U
Salmeterol Xinafoate 6EW8Q962A5
Drug Carriers 0

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

9845

Subventions

Organisme : Jordan Isra University
ID : (RC: 8-43/2020-2021 on 19-8-2021)

Informations de copyright

© 2024. The Author(s).

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Auteurs

Eman Zmaily Dahmash (EZ)

Department of Chemistry and Pharmaceutical Sciences, School of Life Sciences, Pharmacy and Chemistry, Kingston University, London, KT1 2EE, UK. e.dahmash@kingston.ac.uk.

Nour Radwan Achkar (NR)

Department of Applied Pharmaceutical Sciences and Clinical Pharmacy, Faculty Pharmacy, Isra University, Amman, 11622, Jordan.

Dalia Khalil Ali (DK)

Department of Physiotherapy, Faculty of Allied Medical Sciences, Isra University, Amman, 11622, Jordan.

Qais Jarrar (Q)

Department of Applied Pharmaceutical Sciences and Clinical Pharmacy, Faculty Pharmacy, Isra University, Amman, 11622, Jordan.

Affiong Iyire (A)

Aston Pharmacy School, College of Health & Life Sciences, Aston University, Birmingham, B4 7ET, UK.

Shereen M Assaf (SM)

Department of Pharmaceutical Technology, Faculty of Pharmacy, Jordan University of Science and Technology, P. O. Box 3030, Irbid, 22110, Jordan.

Hamad Alyami (H)

Department of Pharmaceutics, College of Pharmacy, Najran University, 55461, Najran, Saudi Arabia.

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Classifications MeSH