Miniaturized active air sampling method for the analysis of tire rubber pollutants from indoor and outdoor places.
air analysis
plasticizers
polycyclic aromatic hydrocarbons
solid-phase extraction
tire rubber
Journal
Journal of separation science
ISSN: 1615-9314
Titre abrégé: J Sep Sci
Pays: Germany
ID NLM: 101088554
Informations de publication
Date de publication:
Apr 2021
Apr 2021
Historique:
revised:
02
02
2021
received:
18
12
2020
accepted:
02
02
2021
pubmed:
11
2
2021
medline:
11
2
2021
entrez:
10
2
2021
Statut:
ppublish
Résumé
An effective, quick, and sustainable air analysis method was developed to analyze 41 volatiles and semivolatile organic compounds present in tire rubber and crumb rubber materials. The proposed method, based on active sampling using a sorbent material followed by an ultrasound assisted extraction, was developed with the aim of obtaining a fast and simple procedure to determine polycyclic aromatic hydrocarbons, plasticizers, antioxidants, and vulcanization agents in air. A small amount of sorbent (25 mg) was used, and the analytes were recovered in only 1 mL of solvent. An experimental design was applied to study the influence of main factors such as type of sorbent and type of solvent, extraction technique (ultrasound-assisted extraction and vortex extraction), extraction time, as well as the factor interactions. Under optimal conditions, no breakthrough occurs in the studied interval (up to 4 m
Identifiants
pubmed: 33566448
doi: 10.1002/jssc.202001249
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
1694-1705Informations de copyright
© 2021 Wiley-VCH GmbH.
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