Preparation of Poly(Ionic Liquid) Particles with Anionic Side Chain by Dispersion Polymerization.
cation exchange
dispersion polymerization
poly(ionic liquid)s
polymer particles
Journal
Macromolecular rapid communications
ISSN: 1521-3927
Titre abrégé: Macromol Rapid Commun
Pays: Germany
ID NLM: 9888239
Informations de publication
Date de publication:
Jul 2020
Jul 2020
Historique:
received:
17
05
2020
revised:
05
06
2020
pubmed:
18
6
2020
medline:
22
6
2021
entrez:
18
6
2020
Statut:
ppublish
Résumé
Micrometer-sized poly(ionic liquid) (PIL) particles with an anionic side chain, poly(1-butyl-3-methylimidazolium 3-sulfopropyl methacrylate) (poly([Bmim][SPMT])), are successfully prepared by dispersion polymerization at 60 °C in ethanol/ethyl acetate (2/8, w/w) with poly(vinylpyrrolidone) as a stabilizer. However, the obtained particles do not maintain the particulate state during drying at room temperature due to poly([Bmim][SPMT])'s low glass-transition temperature, below room temperature. In order to prevent coalescence and maintain particle shape, a cross-linking monomer is added after the nucleation stage of dispersion polymerization. Moreover, Fourier-transform infrared spectroscopy (FT-IR) demonstrates cation exchange between the obtained particles and metal cations (Ag
Identifiants
pubmed: 32548946
doi: 10.1002/marc.202000271
doi:
Substances chimiques
Anions
0
Cations
0
Ionic Liquids
0
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
e2000271Subventions
Organisme : Grant-in-Aid for Scientific Research
ID : 17H03116
Organisme : Japan Society for the Promotion of Science
Organisme : KAKENHI
Informations de copyright
© 2020 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
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