Polysaccharide-Based Chiral Stationary Phases for Enantioseparations by High-Performance Liquid Chromatography: An Overview.

Chromatography, High Pressure Liquid / methods Phenylcarbamates / chemistry Polysaccharides / chemistry Stereoisomerism Temperature
Amylose derivative Cellulose derivative Chiral stationary phase Enantioseparations Polysaccharide phenylcarbamates Polysaccharide-based stationary phase

Journal

Methods in molecular biology (Clifton, N.J.)
ISSN: 1940-6029
Titre abrégé: Methods Mol Biol
Pays: United States
ID NLM: 9214969

Informations de publication

Date de publication:
2019
Historique:
entrez: 10 5 2019
pubmed: 10 5 2019
medline: 23 1 2020
Statut: ppublish

Résumé

This chapter summarizes the application of polysaccharide-based chiral stationary phases (CSPs) for separation of enantiomers in high-performance liquid chromatography (HPLC). Since this book contains dedicated chapters on enantioseparations using supercritical fluid chromatography (SFC), or capillary electrochromatography (CEC), the application of polysaccharide-based materials in these modes of liquid-phase separation techniques is touched just superficially. Special emphasis is directed toward a discussion of the optimization of polysaccharide-based chiral selectors, their attachment onto the carrier, and the optimization of the support. The optimization of the separation of enantiomers based on various parameters such as mobile phase composition and temperature is discussed.

Identifiants

DOI: 10.1007/978-1-4939-9438-0_6 PMID: 31069731
pubmed: 31069731
doi: 10.1007/978-1-4939-9438-0_6
doi:

Substances chimiques

Phenylcarbamates 0
Polysaccharides 0

Types de publication

Journal Article Review

Langues

eng

Sous-ensembles de citation

IM

Pagination

93-126

Auteurs

Bezhan Chankvetadze (B)

Institute of Physical and Analytical Chemistry, School of Exact and Natural Sciences, Tbilisi State University, Tbilisi, Georgia. bezhan_chankvetadze@yahoo.com.

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Classifications MeSH

Recherchemedicale.com › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie en phase liquide à haute performance › Polysaccharide-Based Chiral Stationary Phases...
Recherchemedicale.com › Composés chimiques organiques › Acides carboxyliques › Acides acycliques › Carbamates › Phényl-carbamates › Polysaccharide-Based Chiral Stationary Phases...
Recherchemedicale.com › Glucides › Polyosides › Polysaccharide-Based Chiral Stationary Phases...
Recherchemedicale.com › Phénomènes chimiques › Phénomènes de chimie organique › Isomérie › Stéréoisomérie › Polysaccharide-Based Chiral Stationary Phases...
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